Low-Field Emission from Iron Oxide-Filled Carbon Nanotube Arrays
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摘要:
Arrays of multi-walled carbon nanotubes (MWCNTs) filled with iron oxide have been fabricated by a one-step route based on the pyrolysis of ferrocene under a well-chosen synthesis condition.The MWCNT arrays were observed with a scanning electron microscope, with which an energy dispersive x-ray spectrum (EDXS) was also acquired, and they are analysed by x-ray diffraction.Furthermore, individual MWCNTs were studied by using selected area electron diffraction (SAED) and the EDXS in a transmission electron microscopy observation.All the observation and analysis confirmed that the MWCNTs were filled with iron oxide.Field emission from these arrays of iron oxide-filled MWCNTs was measured and the turn-on field was determined to range from 0.83-1.01 V/μm, appearing to be much lower than those of arrays of pure MWCNTs and arrays of nitrogen-doped MWCNTs fabricated in similar ways.The possible reasons of the observed low-field emission are discussed.