Selective Laser Melting of an Al-Fe-V-Si Alloy: Microstructural Evolution and Thermal Stability
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摘要:
Selective laser melting was used to produce an aluminum alloy Al-8.5Fe-1.3V-1.7Si (wt%).The effects of heat treatment on microstructure evolution and phase stability during long-term thermal exposure of the deposits were investigated.Results show that the microquasi-crystalline phase,Al12(Fe,V)3Si and AlmFe metastable phases coexisted with α-Al in the as-produced alloy.Annealing at 400 ℃ resulted in decomposition of microquasi-crystalline phase and supersaturated α-Al into Al12(Fe,V)3Si phase in the fusion zone,accompanied by the decrease in alloy hardness.The activation energy of this decomposition process was 115 kJ/mol.A more homogenous microstructure was obtained after annealing at 400 ℃ for 60 min,which was resistant to coarsening exposed at 425 ℃ up to 500 h.The Al12(Fe,V)3Si and AlmFe phases were coarsened at 475 and 525 ℃ with increasing the exposure time.Coarsening of Al12(Fe,V)3Si phase was attributed to a combination of volume diffusion and grain boundary diffusion mechanism of Fe.Heat treatment at 600 ℃ resulted in accelerated microstructure coarsening and formation of large-sized equilibrium phases,which significantly degraded the room temperature microhardness.