Microwave Pyrolysis and Electrochemical Supercapacitor of S-doped g-C3N4 Nanoparticles

• 作者: LIU Min-Min HE Na-Ting GUO Hong-Xu YING Shao-Ming CHEN Zhang-Xu
• 来源期刊: 结构化学
• 年，卷（期）: 2021,（6）
• 所属期刊栏目: materials structural chemistry
• 页码范围: 806-810
• 页数: 5页
• 语种: 英文
• DOI: 10.14102/j.cnki.0254-5861.2011-3016

摘要

In this study, S-doped g-C3N4 nanoparticles were successfully prepared by one-step solid-state microwave synthesis. The detailed characterizations through XRD, FT-IR, SEM and XPS were studied. In addition, the electrochemical properties as supercapacitor of the sample were tested by cyclic voltammetry (CV), galvanostatic charge-discharge (GCD) and electrochemical impedance spectroscopy (EIS) techniques. The results showed a high specific capacitance of 691 F/g at current density of 4 A/g in 2 M KOH + 0.15 M K3[Fe(CN)6] electrolyte. This study shows that the microwave synthesis is a promising way to design carbon-based electrodes for supercapacitor.