Synthesis, Characterization and Antibacterial Activity of Mixed Ligand (HL) Complexes Mn(ll), Co(ll), Ni(ll), Zn(ll), Cd(ll) and Hg(ll) with Azide (N<sub>3</sub><sup style="margin-left:-6px;">-</sup>)

• 作者: Dhuha K. Rashid Jassim S. Sultan Sajed M. Lateaf
• 来源期刊: 无机化学期刊(英文)
• 学科: 化学
• 关键词: 4-AMINOANTIPYRINE Glyoxylic Acid Sodium AZIDE SCHIFF Base AZIDO Mixed Ligand
• 年，卷（期）: 2015,（4）
• 页码范围: 102-111
• 页数: 10页
• 分类号: O6

摘要

The complexes of mixed ligand (HL) as primary ligand with azide ion (N3-) as co-ligand with Mn(ll), Co(ll), Ni(ll), Zn(ll), Cd(ll) and Hg(ll) were prepared via reaction metal (ll) chloride salt with ligand (HL) and sodium azide (NaN3) using 1:2:2 mole ratio in ethanol solvent, respectively. The complexes of mixed ligand (HL) were characterized by elemental microanalysis (C.H.N), atomic absorption chloride content, molar conductance, magnetic susceptibility, melting point, FTIR and UV-Vis spectral data. The anti bacterial activity with four kinds of bacteria, Staphylococcus aureus, Bacillus, Escherichia coli and Pseudomonas aureus was studied.